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Case History: Determining contamination in extruded granules

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25
Nov
2013
Category: Laboratory

Case History: Determining contamination in extruded granules

Category: LABORATORY

Understanding your Problem: the need to determine the chemical nature of contaminants present in polyolefin granules.

Providing your Solution: the chemical nature of the contaminant (black colour inclusion) in the granule is determined via FT-IR and DSC analysis.

The IR analysis is performed on the contaminant via ATR with diamond crystal.

 

The analyses performed led us to the following conclusions:

- The IR spectrum compared with the thousands of spectra in our database allowed us to identify the contaminant as being a polyamide.

- The DSC thermal analysis highlighted a melting peak of around 300°C, allowing us to identify the polyamide as  Nylon 4,6 (PA46)

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